Elucidation of crystal growth, structural characterization, thermal properties, and molecular dynamics using NMR near phase transition temperature of [N(CH3)4]2CoCl4

Phase transition temperature

After grinding [N(CH3)4]2CoCl4 single crystals into a fine powder, DSC experiments were performed at a heating rate of 10 °C/min using a sample weight of 2.6 mg. As shown in Fig. 1, three subtle endothermic peaks…

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